2-(Benzyloxy)-1,3-dichlorobenzene synthesis
- Product Name:2-(Benzyloxy)-1,3-dichlorobenzene
- CAS Number:21524-44-7
- Molecular formula:C13H10Cl2O
- Molecular Weight:253.12
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21524-44-7
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$291.00/5g
Yield:21524-44-7 81%
Reaction Conditions:
with di-tert-butyl peroxide;1,3-di-tert-butylimidazolium at 130; for 24 h;Green chemistry;
Steps:
5 Example 5: [(tBuNCH=CHNtBu)CH][FeBr4] catalyzed oxidative coupling reaction of 2,6-dichlorophenol and toluene
Add 2,6-dichlorophenol to the reaction flask one by one(81.5 mg, 0.5 mmol), catalyst (28 mg, 0.05 mmol), di-tert-butyl peroxide (140 μl, 0.75 mmol),Toluene (4.5 ml), react at 130 oC for 24 hours, cool to room temperature after the reaction, and purify the product by column chromatography.(Using petroleum ether as the developing agent), the yield was 81%.
References:
CN112645821,2021,A Location in patent:Paragraph 0026; 0041
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21524-44-7
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$291.00/5g
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21524-44-7
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