(2-BENZYLOXY-PHENYL)-HYDRAZINE HYDROCHLORIDE synthesis
- Product Name:(2-BENZYLOXY-PHENYL)-HYDRAZINE HYDROCHLORIDE
- CAS Number:34288-06-7
- Molecular formula:C13H15ClN2O
- Molecular Weight:250.72
20012-63-9
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Yield:34288-06-7 69%
Reaction Conditions:
Stage #1: o-(benzyloxy)anilinewith hydrogenchloride;sodium nitrite in water at 0;
Stage #2: with hydrogenchloride;tin(ll) chloride in water at 0; for 2 h;
References:
Roullier, Catherine;Chollet-Krugler, Marylne;Weghe, Pierre Van De;Devehat, Franoise Lohezic-Le;Boustie, Joel [Bioorganic and Medicinal Chemistry Letters,2010,vol. 20,# 15,p. 4582 - 4586] Location in patent:experimental part