2-bromo-1-(propan-2-yloxy)ethyl]benzene synthesis
- Product Name:2-bromo-1-(propan-2-yloxy)ethyl]benzene
- CAS Number:63785-56-8
- Molecular formula:C11H15BrO
- Molecular Weight:243.14
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Yield:63785-56-8 87%
Reaction Conditions:
with N,N'-dibromo-N,N'-(1,2-ethanediyl)bis(p-toluenesulfonamide);ammonium acetate at 20; for 0.1 h;
Steps:
Typical Procedure for Bromoether Formation.
General procedure: To a solution of alkene (1 mmol), solvent (alcohols) and NH4OAc (10 mol %), BNBTS (0.6 mmol) was added at room temperature. The reaction was monitored by TlC. After completion of the reaction, the insoluble BNHTS was removed by filtration and washed with Et2O (15 mL) and the organic phase was dried (anhydrous Na2SO4). The solvent was evaporated with a rotatory evaporator, and crude product purified by column chromatography (SiO2; n-Hexane, EtOAc 10:1). The solvent was evaporated to give pure bromoether as colorless or light orange oil.
References:
Kazemi, Foad;Kakroudi, Mazaher Abdollahi [Bulletin of the Korean Chemical Society,2013,vol. 34,# 2,p. 500 - 504]
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67-63-0
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93-52-7
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100-42-5
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67-63-0
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![Benzene, [1-(1-methylethoxy)ethyl]-](/CAS/20180601/GIF/65757-61-1.gif)
65757-61-1
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63785-56-8
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