2-Bromo-3-nitrobenzoyl chloride synthesis
- Product Name:2-Bromo-3-nitrobenzoyl chloride
- CAS Number:6286-36-8
- Molecular formula:C7H3BrClNO3
- Molecular Weight:264.46
573-54-6
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Yield:6286-36-8 100%
Reaction Conditions:
with thionyl chloride for 2 h;Reflux;
Steps:
General synthetic procedure for the title compound 3a-w
General procedure: A mixture of various carboxylic acids (1.0mmol), an excess of thionyl chrolide (5mL) was refluxed for 2h and concentrated in vacuo to give corresponding acyl chloride (quant).
References:
Chen, Yin-Bo;Li, Ji-Ling;Shao, Xu-Sheng;Xu, Xiao-Yong;Li, Zhong [Chinese Chemical Letters,2013,vol. 24,# 8,p. 673 - 676]
603-11-2
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