2'-BROMO-4-METHOXY-BIPHENYL synthesis
- Product Name:2'-BROMO-4-METHOXY-BIPHENYL
- CAS Number:74447-76-0
- Molecular formula:C13H11BrO
- Molecular Weight:263.13
Yield:74447-76-0 97%
Reaction Conditions:
Stage #1: para-iodoanisolewith tert.-butyl lithium in tetrahydrofuran at -78; for 1 h;
Stage #2: with zinc dibromide in tetrahydrofuran at 20; for 0.5 h;
Stage #3: 1-Bromo-2-iodobenzenewith triphenylphosphine;[Pd(dibenzylideneacetone)2] in tetrahydrofuran at 20;
References:
Varela, Jesus A.;Pena, Diego;Goldfuss, Bernd;Denisenko, Dmitri;Kulhanek, Jiri;Polborn, Kurt;Knochel, Paul [Chemistry - A European Journal,2004,vol. 10,# 17,p. 4252 - 4264]
5720-07-0
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![2-(2-Bromophenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborine](/CAS/20180808/GIF/927384-42-7.gif)
927384-42-7
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