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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
152488-38-5

2-Butanol, 1-chloro-3,3-dimethyl-, (2R)- synthesis

5synthesis methods
1-Chloropinacolone

13547-70-1
267 suppliers
$30.00/10g

2-Butanol, 1-chloro-3,3-dimethyl-, (2R)-

152488-38-5
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Yield:90.2 % ee

Reaction Conditions:

with bis(1,5-cyclooctadiene)diiridium(I) dichloride;hydrogen;potassium carbonate;C39H40N3OP in ethanol at 30; under 45004.5 Torr;Autoclave;

References:

Chen, Qian;Sun, Hao;Li, Linlin;Tian, Jie;Xu, Qian;Ma, Nana;Li, Li;Zhang, Lin;Li, Chun [Journal of Organic Chemistry,2022,vol. 87,# 23,p. 15986 - 15997] Location in patent:supporting information

1-Chloropinacolone

13547-70-1
267 suppliers
$30.00/10g

2-Butanol, 1-chloro-3,3-dimethyl-, (S)- (9CI)

152488-36-3
11 suppliers
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2-Butanol, 1-chloro-3,3-dimethyl-, (2R)-

152488-38-5
13 suppliers
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References
2-Butanone, 1,1,1-trichloro-3,3-dimethyl-

36965-30-7
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2-Butanol, 1-chloro-3,3-dimethyl-, (2R)-

152488-38-5
13 suppliers
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References
2-Butanol, 1,1,1-trichloro-3,3-dimethyl-, (2R)-

139040-45-2
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2-Butanol, 1-chloro-3,3-dimethyl-, (2R)-

152488-38-5
13 suppliers
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References
1-chloro-3,3-dimethyl-2-butanol

36402-31-0
5 suppliers
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2-Butanol, 1-chloro-3,3-dimethyl-, (2R)-

152488-38-5
13 suppliers
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References