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ChemicalBook CAS DataBase List 2-CarbaMoyl-3-hydroxy-1,4-naphthoquinone

2-CarbaMoyl-3-hydroxy-1,4-naphthoquinone synthesis

3synthesis methods
Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

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2-CarbaMoyl-3-hydroxy-1,4-naphthoquinone

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 85 percent / NH4OH, NH4Cl / methanol / 2 h / Ambient temperature
2: 64 percent / BCl3 / CH2Cl2 / 24 h / -78 °C

References:

Koyama, Junko;Ogura, Tamaki;Tagahara, Kiyoshi;Konoshima, Takao;Kozuka, Mutsuo [Phytochemistry,1992,vol. 31,# 8,p. 2907 - 2908]

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