2-Chloro-3-iodo-1,4-diMethoxybenzene, 97% synthesis
- Product Name:2-Chloro-3-iodo-1,4-diMethoxybenzene, 97%
- CAS Number:1335243-55-4
- Molecular formula:C8H8ClIO2
- Molecular Weight:298.51
2100-42-7
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1335243-55-4
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$103.00/1g
Yield:1335243-55-4 78%
Reaction Conditions:
Stage #1: 2-chloro-1,4-dimethoxybenzenewith lithium di-tert-butyl(2,2,6,6-tetramethylpiperidino)zincate in tetrahydrofuran at -78 - -30;
Stage #2: with iodine in tetrahydrofuran at -30 - 20;
References:
Guilarte, Veronica;Castroviejo, M. Pilar;Alvarez, Estela;Sanz, Roberto [Beilstein Journal of Organic Chemistry,2011,vol. 7,art. no. 146,p. 1255 - 1260] Location in patent:supporting information; experimental part