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ChemicalBook CAS DataBase List 2-CHLORO-5-NITRONICOTINAMIDE

2-CHLORO-5-NITRONICOTINAMIDE synthesis

9synthesis methods
22280-56-4 Synthesis
2-Chloro-3-methyl-5-nitropyridine

22280-56-4
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: sodium dichromate; sulfuric acid / 15 h / 30 °C
2: thionyl chloride / 3 h / Reflux
3: ammonia / water; acetone / 0.17 h / 25 °C

References:

Beijing Yiling Bioengineering Co., Ltd. EP2366691, 2011, A1

135795-55-0 Synthesis
2-chloro-5-nitronicotinoyl chloride

135795-55-0
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