(2-CHLORO-5-PYRIDYL)METHYLZINC CHLORIDE synthesis
- Product Name:(2-CHLORO-5-PYRIDYL)METHYLZINC CHLORIDE
- CAS Number:352530-36-0
- Molecular formula:C6H5Cl2NZn
- Molecular Weight:227.41
70258-18-3
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352530-36-0
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Yield:-
Reaction Conditions:
Stage #1: 2-chloro-5-(chloromethyl)pyridinewith magnesium;lithium chloride in tetrahydrofuran at 20;Inert atmosphere;Schlenk technique;Heating;
Stage #2: zinc(II) chloride in tetrahydrofuran at 0 - 20;Inert atmosphere;Schlenk technique;
References:
Gra?l, Simon;Hamze, Clémence;Koller, Thadd?us J.;Knochel, Paul [Chemistry - A European Journal,2019,vol. 25,# 15,p. 3752 - 3755] Location in patent:supporting information