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261956-65-4

2-chloro-5-(trifluoromethyl)pyridine 1-oxide synthesis

1synthesis methods
-

Yield:261956-65-4 82%

Reaction Conditions:

with urea hydrogen peroxide adduct;trifluoroacetic anhydride in dichloromethane at 0; for 0.25 h;Oxidation;

References:

Caron, Stéphane;Do, Nga M.;Sieser, Janice E. [Tetrahedron Letters,2000,vol. 41,# 14,p. 2299 - 2302]