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ChemicalBook CAS DataBase List 2-CHLORO-MANDELIC ACID METHYL ESTER
32345-59-8

2-CHLORO-MANDELIC ACID METHYL ESTER synthesis

6synthesis methods
156276-21-0 Synthesis
Methyl 2-(2-chlorophenyl)-2-hydroxyacetate

156276-21-0
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: chromium(VI) oxide; sulfuric acid; water / dichloromethane / 8 h / 0 - 20 °C
2: Bacillus subtilis glucose dehydrogenase; Candida glabrata keto ester reductase No. 1; D-glucose / ethanol / 12 h / 25 °C / pH 6 / aq. phosphate buffer; Enzymatic reaction

References:

Ma, Hongmin;Yang, Linlin;Ni, Yan;Zhang, Jie;Li, Chun-Xiu;Zheng, Gao-Wei;Yang, Huaiyu;Xu, Jian-He [Advanced Synthesis and Catalysis,2012,vol. 354,# 9,p. 1765 - 1772]