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ChemicalBook CAS DataBase List 2-CHLORO-N-(2,3,4,5,6-PENTAFLUOROPHENYL)ACETAMIDE

2-CHLORO-N-(2,3,4,5,6-PENTAFLUOROPHENYL)ACETAMIDE synthesis

1synthesis methods
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Yield:70426-73-2 94%

Steps:

262.A 2-chloro-N-(pentafluorophenyl)acetamide

EXAMPLE 262A 2-chloro-N-(pentafluorophenyl)acetamide The procedure described in Example 22A was followed, substituting pentafluorophenylamine for 3,4,5-trimethoxyaniline to provide the title compound (94% yield) as a tan solid. 1H NMR (300 MHz, DMSO-d6) δ3.31 (s, 2H), 10.48 (br s, 1H); MS (DCI/NH3) m/e 259 (M+H)+; 277 (M+NH4)+.

References:

US2004/29887,2004,A1

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