(2-Chloroethyl)diMethylsulfoniuM iodide synthesis
- Product Name:(2-Chloroethyl)diMethylsulfoniuM iodide
- CAS Number:25059-70-5
- Molecular formula:C4H10ClIS
- Molecular Weight:252.5447
542-81-4
106 suppliers
$72.00/5g
25059-70-5
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$50.00/10 mg
Yield:-
Reaction Conditions:
in methyl iodide
Steps:
2-Chloroethyldimethylsulfonium iodide:
2-Chloroethyldimethylsulfonium iodide: A total of 2.6 g of 2-chloroethylmethylsulfide was dissolved in 10 mL of iodomethane and stirred at room temperature for 2 days. The crude product was filtered and washed by acetone (3*10 mL). 4.2 G of product were obtained after recrystalization from methanol (70%). 1 H NMR (DMSO-d): δ2.98 (s, 6H), 3.80 (t, 2H, J=12.8), 4.13 (t, H, J=12.8).
References:
Rutgers University US5523411, 1996, A
542-81-4
106 suppliers
$72.00/5g
74-88-4
342 suppliers
$15.00/10g
25059-70-5
18 suppliers
$50.00/10 mg