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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
70288-96-9

(2-CHLOROPHENYL)(2-HYDROXYPHENYL)METHANONE synthesis

4synthesis methods
Obtained by total dealkylation of 5-tert-butyl-2?-chloro- 2-methoxybenzophenone with aluminium chloride in benzene at 65–70° for 45 h (60–80%).
95-56-7 Synthesis
2-Bromophenol

95-56-7
313 suppliers
$9.00/5G

(2-CHLOROPHENYL)(2-HYDROXYPHENYL)METHANONE

70288-96-9
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Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: pyridinium p-toluenesulfonate / dichloromethane / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 °C / Inert atmosphere
2.2: 17 h / -78 - 20 °C / Inert atmosphere
3.1: pyridinium p-toluenesulfonate; ethanol / dichloromethane / 20 °C / Inert atmosphere
4.1: manganese(IV) oxide / dichloromethane / 20 °C / Inert atmosphere

References:

Clarkson, Guy J.;Wills, Martin;Zheng, Ye [Organic Letters,2020]

(2-Chlorophenyl)phenyl-methanone

5162-03-8
327 suppliers
$6.00/10g

(2-CHLOROPHENYL)(2-HYDROXYPHENYL)METHANONE

70288-96-9
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References
57999-46-9 Synthesis
2-(2'-BROMOPHENOXY)TETRAHYDRO-2H-PYRAN

57999-46-9
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(2-CHLOROPHENYL)(2-HYDROXYPHENYL)METHANONE

70288-96-9
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References
Methanone, (2-chlorophenyl)[5-(1,1-dimethylethyl)-2-methoxyphenyl]-

103573-58-6
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(2-CHLOROPHENYL)(2-HYDROXYPHENYL)METHANONE

70288-96-9
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References

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