2-cyclobutyl-6-phenylpyridine synthesis
1synthesis methods
- Product Name:2-cyclobutyl-6-phenylpyridine
- CAS Number:1186503-88-7
- Molecular formula:C15H15N
- Molecular Weight:209.29
Yield:1186503-88-7 78%
Reaction Conditions:
Stage #1: 1-azidostyrene;1-cyclobutylcyclopropan-1-olwith manganese(III) acetylacetonate in methanol at 20; for 0.0833333 h;Inert atmosphere;
Stage #2: with acetic acid in methanol at 20; for 0.5 h;
References:
Wang, Yi-Feng;Chiba, Shunsuke [Journal of the American Chemical Society,2009,vol. 131,# 35,p. 12570 - 12572] Location in patent:supporting information; experimental part