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ChemicalBook CAS DataBase List 2-Fluoro-4-Methoxyphenylboronic acid pinacol ester

2-Fluoro-4-Methoxyphenylboronic acid pinacol ester synthesis

3synthesis methods
61676-62-8 Synthesis
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

61676-62-8
310 suppliers
$11.19/5G

2-(2-fluoro-6-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

1599432-41-3
3 suppliers
inquiry

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Yield:1599432-41-3 63%

Reaction Conditions:

Stage #1: 1-fluoro-3-methoxybenzenewith n-butyllithium;N,N,N,N,-tetramethylethylenediamine;diisopropylamine in tetrahydrofuran at -78; for 1.66667 h;Inert atmosphere;
Stage #2: 2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane at -78 - 0;

References:

Wang, Yan;Wang, Le;Chen, Ling-Yan;Bhadury, Pinaki S.;Sun, Zhihua [Australian Journal of Chemistry,2014,vol. 67,# 4,p. 675 - 678]

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