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40105-90-6

2-Furanmethanol, 5-(2-nitrophenyl)- synthesis

3synthesis methods
-

Yield:40105-90-6 99%

Reaction Conditions:

Stage #1: 5-(2-nitrophenyl)-2-furaldehydewith sodium tetrahydroborate in methanol at 20; for 2 h;
Stage #2: with water in methanol;

References:

Hashmi, A. Stephen K.;Rudolph, Matthias;Huck, Juergen;Frey, Wolfgang;Bats, Jan W.;Hamzic, Melissa [Angewandte Chemie - International Edition,2009,vol. 48,# 32,p. 5848 - 5852] Location in patent:supporting information; experimental part