ChemicalBook CAS DataBase List 2-hydroxy-6-(methoxymethoxy)benzaldehyde

2-hydroxy-6-(methoxymethoxy)benzaldehyde synthesis

8synthesis methods

Product Name:2-hydroxy-6-(methoxymethoxy)benzaldehyde
CAS Number:84290-49-3
Molecular formula:C9H10O4
Molecular Weight:182.17

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2-hydroxy-6-(methoxymethoxy)benzaldehyde

84290-49-3
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane / 2 h / -10 °C / Inert atmosphere
1.2: 1 h / 0 °C / Inert atmosphere
2.1: hydrogenchloride / water; tetrahydrofuran / 1.5 h / Inert atmosphere

References:

GLOBAL BLOOD THERAPEUTICS, INC.;LI, Zhe WO2015/31285, 2015, A1

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84290-49-3
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References

4H-1,3-Benzodioxin-4-one, 5-(methoxymethoxy)-2,2-dimethyl-

888958-28-9
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84290-49-3
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References

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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References

6751-75-3 Synthesis

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References