ChemicalBook CAS DataBase List 2-iodo-1-methoxy-3-methylbenzene

2-iodo-1-methoxy-3-methylbenzene synthesis

3synthesis methods

Product Name:2-iodo-1-methoxy-3-methylbenzene
CAS Number:35387-94-1
Molecular formula:C8H9IO
Molecular Weight:248.06

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Yield:35387-94-1 78%

Reaction Conditions:

Stage #1: 2-methoxy-6-methylbenzeneaminewith hydrogenchloride;sodium nitrite in water at 0; for 1 h;Diazotization;
Stage #2: with potassium iodide in water at 25; for 12 h;Further stages.;Iodination;Sandmeyer reaction;

References:

Coleman;Guernon;Roland [Organic letters,2000,vol. 2,# 3,p. 277 - 280]

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References

100-84-5 Synthesis

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References

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