2-iodo-3-nitrobenzonitrile synthesis
- Product Name:2-iodo-3-nitrobenzonitrile
- CAS Number:1261481-69-9
- Molecular formula:C7H3IN2O2
- Molecular Weight:274.02
87331-46-2
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1261481-69-9
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Yield:-
Reaction Conditions:
Stage #1:2-amino-3-nitrobenzonitrile with hydrogenchloride;sodium nitrite in water at 0 - 5; for 0.5 h;Sandmeyer Reaction;
Stage #2: with potassium iodide in water at 5 - 20; for 4 h;Sandmeyer Reaction;
References:
Praveen, Chandrasekaran;Dheenkumar;Perumal [Journal of Chemical Sciences,2013,vol. 125,# 1,p. 71 - 83]