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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
4696-14-4

2-ISO-PROPYLIDENEBICYCLO[2.2.1]HEPTANE synthesis

10synthesis methods
Ethanone, 1-[3-(trimethylsilyl)bicyclo[2.2.1]hept-5-en-2-yl]-, (2-endo,3-exo)- (9CI)

123334-90-7
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2-ISO-PROPYLIDENEBICYCLO[2.2.1]HEPTANE

4696-14-4
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-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 99 percent / H2 / 10percent Pd on C / diethyl ether / 2 h
2: 95 percent / diethyl ether / 2 h / -78 °C
3: 76 percent / BF3*2AcOH / CH2Cl2 / 0.25 h / 0 °C

References:

Fleming, Ian;Patel, Shailesh K.;Urch, Christopher J. [Journal of the Chemical Society. Perkin transactions I,1989,p. 115 - 124]

Diethyl ether

60-29-7
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$31.19/50g

Ethanone, 1-bicyclo[2.2.1]hept-1-yl-

80606-49-1
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2-ISO-PROPYLIDENEBICYCLO[2.2.1]HEPTANE

4696-14-4
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Bicyclo[2.2.1]heptane-2-methanol, α,α-dimethyl-3-(trimethylsilyl)-, (2-endo,3-exo)- (9CI)

79239-06-8
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2-ISO-PROPYLIDENEBICYCLO[2.2.1]HEPTANE

4696-14-4
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Hydrochloric acid-D，DCL20WT%

769-85-7
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2-ISO-PROPYLIDENEBICYCLO[2.2.1]HEPTANE

4696-14-4
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Bicyclo[2.2.1]heptan-2-ol, 2-(1-methylethyl)-

83926-65-2
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2-ISO-PROPYLIDENEBICYCLO[2.2.1]HEPTANE

4696-14-4
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References