2-Methoxy-5-phenylphenol synthesis
- Product Name:2-Methoxy-5-phenylphenol
- CAS Number:37055-80-4
- Molecular formula:C13H12O2
- Molecular Weight:200.23
613-37-6
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37055-80-4
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$338.00/1g
Yield:37055-80-4 83%
Reaction Conditions:
Stage #1: 4-methoxylbiphenylwith (TMP)2Cu(CN)Li2 in tetrahydrofuran at -78 - 0; for 2 h;Inert atmosphere;Schlenk technique;
Stage #2: with tert.-butylhydroperoxide in tetrahydrofuran;decane at -78; for 0.5 h;Inert atmosphere;Schlenk technique;regioselective reaction;
References:
Tezuka, Noriyuki;Shimojo, Kohei;Hirano, Keiichi;Komagawa, Shinsuke;Yoshida, Kengo;Wang, Chao;Miyamoto, Kazunori;Saito, Tatsuo;Takita, Ryo;Uchiyama, Masanobu [Journal of the American Chemical Society,2016,vol. 138,# 29,p. 9166 - 9171] Location in patent:supporting information
![[1,1'-Biphenyl]-3-ol, 4-methoxy-, 3-acetate](/CAS/20210305/GIF/92549-29-6.gif)
92549-29-6
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37055-80-4
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148-86-7
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37055-80-4
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92-69-3
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37055-80-4
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14031-80-2
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37055-80-4
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