ChemicalBook CAS DataBase List 2-Methoxy-5-phenylphenol

2-Methoxy-5-phenylphenol synthesis

10synthesis methods

Product Name:2-Methoxy-5-phenylphenol
CAS Number:37055-80-4
Molecular formula:C13H12O2
Molecular Weight:200.23

613-37-6 Synthesis

613-37-6
120 suppliers
$25.00/5g

37055-80-4
12 suppliers
$338.00/1g

Yield:37055-80-4 83%

Reaction Conditions:

Stage #1: 4-methoxylbiphenylwith (TMP)2Cu(CN)Li₂ in tetrahydrofuran at -78 - 0; for 2 h;Inert atmosphere;Schlenk technique;
Stage #2: with tert.-butylhydroperoxide in tetrahydrofuran;decane at -78; for 0.5 h;Inert atmosphere;Schlenk technique;regioselective reaction;

References:

Tezuka, Noriyuki;Shimojo, Kohei;Hirano, Keiichi;Komagawa, Shinsuke;Yoshida, Kengo;Wang, Chao;Miyamoto, Kazunori;Saito, Tatsuo;Takita, Ryo;Uchiyama, Masanobu [Journal of the American Chemical Society,2016,vol. 138,# 29,p. 9166 - 9171] Location in patent:supporting information

[1,1'-Biphenyl]-3-ol, 4-methoxy-, 3-acetate

92549-29-6
0 suppliers
inquiry

37055-80-4
12 suppliers
$338.00/1g

References

148-86-7
72 suppliers
$11.00/5g

37055-80-4
12 suppliers
$338.00/1g

References

92-69-3 Synthesis

92-69-3
410 suppliers
$6.00/25g

37055-80-4
12 suppliers
$338.00/1g

References

14031-80-2
13 suppliers
inquiry

37055-80-4
12 suppliers
$338.00/1g

References