ChemicalBook CAS DataBase List 2-METHOXY-BENZENE-1,3,5-TRIOL

2-METHOXY-BENZENE-1,3,5-TRIOL synthesis

4synthesis methods

Product Name:2-METHOXY-BENZENE-1,3,5-TRIOL
CAS Number:487-71-8
Molecular formula:C7H8O4
Molecular Weight:156.14

487-70-7 Synthesis

487-70-7
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487-71-8
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Cooling with ice
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane; water / 20 °C
3: potassium carbonate / acetone / 56 °C / Inert atmosphere
4: hydrogenchloride / water; methanol / 20 °C

References:

Chao, Shi-Wei;Su, Ming-Yuan;Chiou, Lih-Chu;Chen, Liang-Chieh;Chang, Chung-I;Huang, Wei-Jan [Journal of Natural Products,2015,vol. 78,# 8,p. 1969 - 1976]

606-35-9
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487-71-8
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References

100860-46-6
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487-71-8
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References

212265-19-5
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487-71-8
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References

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