(2-methyl-1,3-benzothiazol-5-yl)methanamine synthesis
- Product Name:(2-methyl-1,3-benzothiazol-5-yl)methanamine
- CAS Number:903630-23-9
- Molecular formula:C9H10N2S
- Molecular Weight:178.2541
68867-14-1
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: pyridine / dichloromethane / 12 h / 0 - 20 °C
2: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; sodium carbonate / 1,4-dioxane; water / 24 h / Reflux
3: ethylenediamine / 1,4-dioxane; propan-1-ol; water / 24 h / Reflux
References:
Murai, Norio;Miyano, Masayuki;Yonaga, Masahiro;Tanaka, Keigo [Organic Letters,2012,vol. 14,# 11,p. 2818 - 2821]
1006-99-1
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611235-48-4
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903630-23-9
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