2-Methyl-2'-deoxyadenosine synthesis
- Product Name:2-Methyl-2'-deoxyadenosine
- CAS Number:110952-90-4
- Molecular formula:C11H15N5O3
- Molecular Weight:265.27
75-24-1
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118706-49-3
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110952-90-4
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Yield:110952-90-4 70%
Reaction Conditions:
Stage #1: 2-iodo-9-<2-deoxy-β-D-ribofuranosyl>adeninewith ammonium sulfate;1,1,1,3,3,3-hexamethyl-disilazane at 40; for 0.333333 h;
Stage #2: trimethylaluminumwith tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran;toluene at 60;Inert atmosphere;
References:
Matyasovsky, Ján;Perlikova, Pavla;Malnuit, Vincent;Pohl, Radek;Hocek, Michal [Angewandte Chemie - International Edition,2016,vol. 55,# 51,p. 15856 - 15859][Angew. Chem.,2016,vol. 128,p. 16088 - 16091,4] Location in patent:supporting information
68498-25-9
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110952-90-4
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![[2,4'-Bi-1H-imidazol]-5'-amine, 1'-(2-deoxy-β-D-erythro-pentofuranosyl)-](/CAS/20210305/GIF/151229-13-9.gif)
151229-13-9
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110952-90-4
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958-09-8
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$5.00/1g
110952-90-4
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951-78-0
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$5.00/100mg
1445-08-5
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$360.00/1G
110952-90-4
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