2-Morpholinobenzo[d]thiazol-6-aMine synthesis
- Product Name:2-Morpholinobenzo[d]thiazol-6-aMine
- CAS Number:850021-27-1
- Molecular formula:C11H13N3OS
- Molecular Weight:235.31
423738-98-1
8 suppliers
inquiry
850021-27-1
22 suppliers
inquiry
Yield:850021-27-1 98%
Reaction Conditions:
with acetic acid;zinc in ethanol; for 0.5 h;Reflux;
Steps:
General procedure for the synthesis of Triazolbenzo[d]thiazoles
General procedure: 1a-c/2a-c or 14 (0.77 mmol) was added to a dry round-bottom flask in THF (7 ml) followed by CuI (0.77 mmol), DIPEA (2.31 mmol) and alkyne (1.16 mmol). The solution was allowed to stir at room temperature until starting material was consumed 1- 10 hrs. The reaction mixture was concentrated, purified by flash chromatography to afford the targeted Triazolbenzo[d]thiazoles.
References:
Avila, Belem;Roth, Aaron;Streets, Heather;Kurth, Mark J.;Dwyer, Donard S. [Bioorganic and medicinal chemistry letters,2012,vol. 22,# 18,p. 5976 - 5978,3] Location in patent:supporting information
110-91-8
675 suppliers
$9.00/1g
2406-90-8
102 suppliers
$65.00/500mg
850021-27-1
22 suppliers
inquiry
6285-57-0
197 suppliers
$9.00/1g
850021-27-1
22 suppliers
inquiry
2407-11-6
108 suppliers
$9.00/250mg
850021-27-1
22 suppliers
inquiry