2-naphthylmethyl acrylate synthesis
- Product Name:2-naphthylmethyl acrylate
- CAS Number:93359-80-9
- Molecular formula:C14H12O2
- Molecular Weight:212.24
Yield:93359-80-9 94%
Reaction Conditions:
Stage #1: 2-Naphthalenemethanolwith dmap;triethylamine in dichloromethane at 0;Schlenk technique;
Stage #2: acryloyl chloride in dichloromethane at 0 - 20; for 4 h;Schlenk technique;
References:
Yamamoto, Eiji;Hilton, Margaret J.;Orlandi, Manuel;Saini, Vaneet;Toste, F. Dean;Sigman, Matthew S. [Journal of the American Chemical Society,2016,vol. 138,# 49,p. 15877 - 15880] Location in patent:supporting information
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