2-PHENOXYETHYLAMINEHCL synthesis
- Product Name:2-PHENOXYETHYLAMINEHCL
- CAS Number:17959-64-7
- Molecular formula:C8H12ClNO
- Molecular Weight:173.64
921596-28-3
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17959-64-7
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Yield:-
Reaction Conditions:
with hydrogenchloride in ethyl acetate at 20; for 0.25 h;
Steps:
31.2
Step 2: Hydrochloride salt of 2-phenoxyethanamine; To tert-butyl (2-phenoxyethyl)carbamate added ethyl acetate HCl and stirred at room temperature for 15 mins. Then ethyl acetate was evaporated and the product was dried and used for next step. 1H NMR (CDCl3) δ 8.16 (m, 2H); 7.30 (t, 2H, J= 15.3 Hz); 6.96 (d, 3H5 J = 8.4 Hz); 4.16 (t, 2H, J= 9.3 Hz); 3.19 (m, 2H)
References:
WO2010/7482,2010,A2 Location in patent:Page/Page column 35
1758-46-9
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17959-64-7
14 suppliers
$101.00/1g