2-Propenoic acid (3-methoxyphenyl)methyl ester synthesis
- Product Name:2-Propenoic acid (3-methoxyphenyl)methyl ester
- CAS Number:144261-46-1
- Molecular formula:C11H12O3
- Molecular Weight:192.21
6971-51-3
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Yield: 40%
Reaction Conditions:
Stage #1:3-methoxybenzyl alcohol with dmap;triethylamine in dichloromethane at 0;Schlenk technique;
Stage #2:acryloyl chloride in dichloromethane at 0 - 20; for 4 h;Schlenk technique;
References:
Yamamoto, Eiji;Hilton, Margaret J.;Orlandi, Manuel;Saini, Vaneet;Toste, F. Dean;Sigman, Matthew S. [Journal of the American Chemical Society,2016,vol. 138,# 49,p. 15877 - 15880] Location in patent:supporting information