2-Styrylquinoline synthesis
- Product Name:2-Styrylquinoline
- CAS Number:4945-26-0
- Molecular formula:C17H13N
- Molecular Weight:231.29
Yield:4945-26-0 96 %Chromat.
Reaction Conditions:
in 1-methyl-pyrrolidin-2-one at 160; under 4500.45 Torr;Glovebox;Autoclave;Solvent;Pressure;
Steps:
1-40
In the glove box, add benzylamine (1.0mmol), 2-methylquinoline (2.0mmol) and NMP (2.0mL) to a dry reaction vial with a magnetic stirrer, place the reaction vial in an autoclave, Fill the autoclave with air (6 bar).Place the autoclave in a preheated metal bath and react at 160°C for 24h.The reaction was stopped, and n-hexadecane was added as an internal standard, and the GC yield was 96%.
References:
CN115611799,2023,A Location in patent:Paragraph 0033-0052
91-63-4
268 suppliers
$23.00/25g
100-51-6
1358 suppliers
$5.00/100g
4945-26-0
4 suppliers
inquiry
1613-41-8
2 suppliers
inquiry
1613-41-8
2 suppliers
inquiry
4945-26-0
4 suppliers
inquiry
