![](/CAS/GIF/131470-66-1.gif)
2-(TRIBUTYLSTANNYL)-5,6-DIHYDRO-[1,4]-DIOXIN synthesis
- Product Name:2-(TRIBUTYLSTANNYL)-5,6-DIHYDRO-[1,4]-DIOXIN
- CAS Number:131470-66-1
- Molecular formula:C16H32O2Sn
- Molecular Weight:375.13
![1,4-DIOXENE](/CAS/GIF/543-75-9.gif)
543-75-9
60 suppliers
$60.00/100mg
![Tributyltin chloride](/CAS/GIF/1461-22-9.gif)
1461-22-9
204 suppliers
$10.00/10g
![2-(TRIBUTYLSTANNYL)-5,6-DIHYDRO-[1,4]-DIOXIN](/CAS/GIF/131470-66-1.gif)
131470-66-1
9 suppliers
inquiry
Yield:131470-66-1 94%
Reaction Conditions:
Stage #1: 1,4-dioxenewith tert.-butyl lithium in diethyl ether;pentane at -78 - -40; for 0.5 h;
Stage #2: tributyltin chloride in diethyl ether;pentane at 10; for 1 h;
References:
Kravina, Alberto G.;Carreira, Erick M. [Angewandte Chemie - International Edition,2018,vol. 57,# 40,p. 13159 - 13162][Angew. Chem.,2018,vol. 130,# 40,p. 13343 - 13346,4] Location in patent:supporting information