ChemicalBook CAS DataBase List 2-UNDECENOIC ACID

2-UNDECENOIC ACID synthesis

8synthesis methods

Product Name:2-UNDECENOIC ACID
CAS Number:15790-94-0
Molecular formula:C11H20O2
Molecular Weight:184.28

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15790-94-0
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$31.39/1g

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: Zn(2,2,6,6-tetramethylpiperidine)_2*2LiCl; zinc(II) chloride / tetrahydrofuran / 1.5 h / -40 °C / Inert atmosphere; Sealed tube
1.2: 12 h / -40 - 60 °C / Inert atmosphere; Sealed tube
2.1: ozone / acetone / 1 h / -78 °C / Inert atmosphere
2.2: 5 h / 0 - 20 °C / Inert atmosphere
3.1: Zn(2,2,6,6-tetramethylpiperidine)_2*2LiCl; zinc(II) chloride / tetrahydrofuran / 1.5 h / -40 °C / Inert atmosphere; Sealed tube
3.2: 12 h / -40 - 60 °C / Inert atmosphere; Sealed tube

References:

Zhao, Yizhou;Chen, Yifeng;Newhouse, Timothy R. [Angewandte Chemie - International Edition,2017,vol. 56,# 42,p. 13122 - 13125][Angew. Chem.,2017,vol. 129,# 42,p. 13302 - 13305,4]