ChemicalBook CAS DataBase List 2-ACETAMIDO-3,4,6-TRI-O-ACETYL-2-DEOXY-BETA-D-GLUCOPYRANOSYL ISOTHIOCYANATE

2-ACETAMIDO-3,4,6-TRI-O-ACETYL-2-DEOXY-BETA-D-GLUCOPYRANOSYL ISOTHIOCYANATE synthesis

4synthesis methods

Product Name:2-ACETAMIDO-3,4,6-TRI-O-ACETYL-2-DEOXY-BETA-D-GLUCOPYRANOSYL ISOTHIOCYANATE
CAS Number:20590-45-8
Molecular formula:C15H20N2O8S
Molecular Weight:388.39

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α-D-Glucopyranosyl bromide, 2-(acetylamino)-2-deoxy-, 3,4,6-triacetate

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2-ACETAMIDO-3,4,6-TRI-O-ACETYL-2-DEOXY-BETA-D-GLUCOPYRANOSYL ISOTHIOCYANATE

20590-45-8
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$45.00/10mg

Yield:20590-45-8 116 mg

Reaction Conditions:

Stage #1: potassium thioacyanatewith 4 A molecular sieve;tetra(n-butyl)ammonium hydrogensulfate in acetonitrile at 20; for 3 h;
Stage #2: 2-acetylamino-3,4,6-triacetyl-2-deoxy-α-D-glucopyranosyl bromide in acetonitrile at 65; for 1.5 h;Further stages.;

References:

Liav, Avraham;Angala, Shiva K.;Brennan, Patrick J. [Synthetic Communications,2008,vol. 38,# 8,p. 1176 - 1183]

333-20-0
426 suppliers
$13.50/100G