Pentanoic acid, 4-[[(1,1-dimethylethoxy)carbonyl]amino]-, (4S)- (9CI) synthesis
- Product Name:Pentanoic acid, 4-[[(1,1-dimethylethoxy)carbonyl]amino]-, (4S)- (9CI)
- CAS Number:207924-92-3
- Molecular formula:C10H19NO4
- Molecular Weight:217.26
28875-17-4
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207924-92-3
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: DIBAL-H / toluene; methanol / 0.5 h / -78 °C
1.2: 72 percent / toluene / 12 h / -78 °C
2.1: 61 percent / 10 percent aq. NaOH / methanol / 18 h / 20 °C
3.1: 100 percent / H2 / 10 percent Pd/C / ethyl acetate / 3 h / 2327.17 Torr
References:
Yang, Hua;Jurkauskas, Valdas;Mackintosh, Nicole;Mogren, Tobias;Stephenson, Corey R. J.;Foster, Katherine;Brown, William;Roberts, Edward [Canadian Journal of Chemistry,2000,vol. 78,# 6,p. 800 - 808]
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142723-69-1
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1000210-73-0
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207924-92-3
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![Pentanoic acid, 4-[[(1,1-dimethylethoxy)carbonyl]amino]-, methyl ester, (4S)-](/CAS/20210305/GIF/186903-41-3.gif)
186903-41-3
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207924-92-3
61 suppliers
$50.00/10 mg
1000210-73-0
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207924-92-3
61 suppliers
$50.00/10 mg