ethyl 4-(3-bromophenyl)-6-methyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate synthesis
- Product Name:ethyl 4-(3-bromophenyl)-6-methyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
- CAS Number:294854-53-8
- Molecular formula:C14H15BrN2O2S
- Molecular Weight:355.25
3132-99-8
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Yield:294854-53-8 90%
Reaction Conditions:
with sulfuric acid immobilized on activated charcoal in hexane;acetonitrile; for 0.833333 h;Reflux;Biginelli pyrimidine synthesis;
References:
Dilmaghani, Karim Akbari;Zeynizadeh, Behzad;Parasajam, Hadi [Phosphorus, Sulfur and Silicon and the Related Elements,2012,vol. 187,# 4,p. 544 - 553] Location in patent:experimental part