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296237-49-5

6H-Benzofuro[3a,3,2-ef][2]benzazepin-6-one, 4a,5,9,10,11,12-hexahydro-3-methoxy-11-methyl- synthesis

5synthesis methods
Spiro[6H-benzofuro[3a,3,2-ef][2]benzazepine-6,2'-[1,3]dioxolane]-11(12H)-carboxaldehyde, 1-bromo-4a,5,9,10-tetrahydro-3-methoxy-4'-methyl-

252869-10-6
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6H-Benzofuro[3a,3,2-ef][2]benzazepin-6-one, 4a,5,9,10,11,12-hexahydro-3-methoxy-11-methyl-

296237-49-5
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inquiry

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Yield:296237-49-5 95%

Reaction Conditions:

with hydrogenchloride;lithium aluminium tetrahydride;air

References:

Czollner, Laszlo;Frantsits, Werner;Kueenburg, Bernhard;Hedenig, Ursula;Froehlich, Johannes;Jordis, Ulrich [Tetrahedron Letters,1998,vol. 39,# 15,p. 2087 - 2088]