2H-Indol-2-one,1,3-dihydro-5-(1-methylethyl)-(9CI) synthesis
- Product Name:2H-Indol-2-one,1,3-dihydro-5-(1-methylethyl)-(9CI)
- CAS Number:156232-25-6
- Molecular formula:C11H13NO
- Molecular Weight:175.23
1168722-73-3
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Yield:156232-25-6 99%
Reaction Conditions:
with hydrogen;palladium on activated charcoal in methanol; under 760.051 Torr; for 3 h;
Steps:
A127.A
5-isopropenylindolin-2-one (15 mg, 0.0866 mmol) was then dissolved into MeOH and the solution purged with N2 (g). 2 mg of 10 % Pd/C (Degussa type) was then added and the mixture purged briefly with H2 (g). The mixture was stirred under 1 atm of H2 (g>for 3 hours and then filtered through a pad of celite. The solvent was removed to give 15 mg, 99 % of the product as an off-white solid. MS ESI 176.0 [M + H]+, calcd for [C11H13NO + H]+ 176.11
References:
WO2009/79767,2009,A1 Location in patent:Page/Page column 189
150560-58-0
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99-88-7
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![Acetamide, 2-(hydroxyimino)-N-[4-(1-methylethyl)phenyl]-](/CAS/20180529/GIF/68701-52-0.gif)
68701-52-0
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