(2S,3S)-1,4-Dichlorobutane-diol Sulfate synthesis
- Product Name:(2S,3S)-1,4-Dichlorobutane-diol Sulfate
- CAS Number:190850-76-1
- Molecular formula:C4H6Cl2O4S
- Molecular Weight:221.06
139165-54-1
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$110.50/50mg
190850-76-1
14 suppliers
$125.00/50mg
Yield:190850-76-1 93%
Reaction Conditions:
Stage #1: (2S,3S)-1,4-dichlorobutan-2,3-diolwith thionyl chloride in tetrachloromethane; for 0.5 h;Heating;
Stage #2: with ruthenium trichloride;sodium periodate in tetrachloromethane;water;acetonitrile at 0; for 1 h;Further stages.;
References:
Kim;Bae;So;Yoo;Chang;Lee;Kang [Organic letters,2001,vol. 3,# 15,p. 2349 - 2351]