ChemicalBook CAS DataBase List (2S,3S)-FMoc-Abu(3-N3)-OH

(2S,3S)-FMoc-Abu(3-N3)-OH synthesis

1synthesis methods

Product Name:(2S,3S)-FMoc-Abu(3-N3)-OH
CAS Number:131669-42-6
Molecular formula:C19H18N4O4
Molecular Weight:366.3706

73731-37-0 Synthesis

2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-hydroxy-butanoic acid

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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 84 percent / N,N-bis(2-oxo-3-oxazolidinyl)phosphordiamidic chloride, EtN(i-Pr)2 / CH₂Cl₂ / 16 h / 0 deg C to r.t.
2: PPh₃, HN₃, diethyl azodicarboxylate / dimethylformamide; toluene / 6 h / Ambient temperature
3: 81 percent / 7N HCl / dioxane / 16 h / 80 °C

References:

Schmidt;Mundinger;Riedl;Haas;Lau [Synthesis,1992,# 12,p. 1201 - 1202]