
3-(1,1-dioxothiomorpholin-4-yl)phenylamine synthesis
- Product Name:3-(1,1-dioxothiomorpholin-4-yl)phenylamine
- CAS Number:1152859-34-1
- Molecular formula:C10H14N2O2S
- Molecular Weight:226.3

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Yield:-
Steps:
Multi-step reaction with 3 steps
1: potassium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / Reflux
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 10 - 15 °C
3: hydrogen / palladium 10% on activated carbon / methanol / Inert atmosphere
References:
WO2012/59932,2012,A1

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