ChemicalBook CAS DataBase List 3-(1,1-dioxothiomorpholin-4-yl)phenylamine

3-(1,1-dioxothiomorpholin-4-yl)phenylamine synthesis

2synthesis methods

Product Name:3-(1,1-dioxothiomorpholin-4-yl)phenylamine
CAS Number:1152859-34-1
Molecular formula:C10H14N2O2S
Molecular Weight:226.3

585-79-5 Synthesis

585-79-5
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3-(1,1-dioxothiomorpholin-4-yl)phenylamine

1152859-34-1
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: potassium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / Reflux
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 10 - 15 °C
3: hydrogen / palladium 10% on activated carbon / methanol / Inert atmosphere

References:

WO2012/59932,2012,A1

1374585-72-4
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1152859-34-1
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References

3-(1,1-dioxothiomorpholin-4-yl)phenylamine Related Search:

4-(dimethylamino)-2-butanone hydrochloride 4-(4-BROMOPHENYL)-2-AZETIDINONE 1,3-dihydro-3-ethyl-2H-indol-2-one

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