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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
15448-75-6

3-(1-Methylethenyl)-2,5-dimethyl-3,4-hexadien-2-ol synthesis

2synthesis methods
Boroxin, 2,4,6-tris(1-methylethenyl)-

14559-92-3
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2,5-Dimethyl-3-hexyne-2,5-diol

142-30-3
295 suppliers
$8.00/25g

3-(1-Methylethenyl)-2,5-dimethyl-3,4-hexadien-2-ol

15448-75-6
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Yield:15448-75-6 57%

Reaction Conditions:

with pyridine;tetrakis(triphenylphosphine) palladium(0) in toluene at 55; for 72 h;Schlenk technique;Inert atmosphere;

References:

Green, Nicholas J.;Willis, Anthony C.;Sherburn, Michael S. [Angewandte Chemie - International Edition,2016,vol. 55,# 32,p. 9244 - 9248][Angew. Chem.,2016,vol. 128,# 32,p. 9390 - 9394] Location in patent:supporting information

5-Isopropylidene-2,2,4,4-tetramethyl-1-oxaspiro[2.2]pentane

15448-69-8
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3-(1-Methylethenyl)-2,5-dimethyl-3,4-hexadien-2-ol

15448-75-6
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References