3-(1-PYRROLIDINYL)-PIPERIDINE synthesis
- Product Name:3-(1-PYRROLIDINYL)-PIPERIDINE
- CAS Number:144243-28-7
- Molecular formula:C9H18N2
- Molecular Weight:154.25
72692-99-0
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$90.00/500mg
144243-28-7
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$174.16/0.5g
Yield:144243-28-7 93%
Reaction Conditions:
Stage #1: 3-(1H-pyrrol-1-yl)pyridinewith hydrogenchloride;palladium 10% on activated carbon;hydrogen in methanol;water at 100; under 53203.6 Torr; for 8 h;Autoclave;
Stage #2: with sodium hydrogencarbonate in isopropyl alcohol; for 1.5 h;Reflux;
References:
Smaliy;Chaykovskaya;Yurchenko;Lakhtadyr;Yurchenko;Shtil;Kostuk [Chemistry of Heterocyclic Compounds,2011,vol. 47,# 9,p. 1178 - 1179] Location in patent:experimental part