3-(3-BroMophenyl)benzo[d]isoxazole synthesis
3synthesis methods
- Product Name:3-(3-BroMophenyl)benzo[d]isoxazole
- CAS Number:99763-25-4
- Molecular formula:C13H8BrNO
- Molecular Weight:274.11
Yield:99763-25-4 78%
Reaction Conditions:
Stage #1: 3-bromo-N-hydroxybenzimidoyl chloride;2-(trimethylsilyl)phenyl trifluoromethanesulfonate in tetrahydrofuran at 20; for 0.0833333 h;
Stage #2: with tetrabutyl ammonium fluoride in tetrahydrofuran at 20; for 0.00833333 h;
References:
Spiteri, Christian;Sharma, Pallavi;Zhang, Fengzhi;MacDonald, Simon J. F.;Keeling, Steve;Moses, John E. [Chemical Communications,2010,vol. 46,# 8,p. 1272 - 1274] Location in patent:supporting information; experimental part
