3,3-DIFLUOROCYCLOBUTANAMINE HYDROCHLORIDE synthesis
- Product Name:3,3-DIFLUOROCYCLOBUTANAMINE HYDROCHLORIDE
- CAS Number:637031-93-7
- Molecular formula:C4H8ClF2N
- Molecular Weight:143.56
791061-00-2
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$8.00/250mg
637031-93-7
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$6.00/100mg
Yield:637031-93-7 95%
Reaction Conditions:
with hydrogenchloride in ethanol;water at 10 - 15; for 8 h;Solvent;
Steps:
7; 8 Example 7: Synthesis of Compound 6
Add compound 5 (90g, 0.84mol) synthesized in Example 4 to a 250mL reaction flask, add 4M hydrochloric acid ethanol solution (540g) at 10-15°C, stir for 8 hours, concentrate under reduced pressure to dryness, add ethyl acetate ( 450 mL) was stirred for 1 hour, then filtered and dried in vacuum at 50°C to obtain 114.3 g of a white solid with a yield of 95% and a purity of 100%.
References:
CN112279785, 2021, A Location in patent:Paragraph 0034; 0062-0065
939399-53-8
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637031-93-7
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107496-54-8
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86770-82-3
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1029720-19-1
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637031-93-7
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$6.00/100mg