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ChemicalBook CAS DataBase List 3,3-DIMETHYL-1-BUTENYLBORONIC ACID
86595-37-1

3,3-DIMETHYL-1-BUTENYLBORONIC ACID synthesis

5synthesis methods
-

Yield:86595-37-1 93%

Reaction Conditions:

with water in diethyl ether;dichloromethane;under N2; to excess of H2O in Et2O added cooled (0 °C) soln. of B complex in CH2Cl2 with stirring, stirred for 10 min; water layer sepd., org. layer washed with cold H2O and brine, dried with MgSO4, evapd. in vac., recrystd. from C6H6;

References:

Brown, Herbert C.;Bhat;Somayaji, Vishwanatha [Organometallics,1983,vol. 2,# 10,p. 1311 - 1316]