3,3-DIMETHYL-1-BUTENYLBORONIC ACID synthesis
- Product Name:3,3-DIMETHYL-1-BUTENYLBORONIC ACID
 - CAS Number:86595-37-1
 - Molecular formula:C6H13BO2
 - Molecular Weight:127.98
 
                        
                        72228-60-5
                        
                        
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                        86595-37-1
                        
                        
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Yield:86595-37-1 93%
Reaction Conditions:
with water in diethyl ether;dichloromethane;under N2; to excess of H2O in Et2O added cooled (0 °C) soln. of B complex in CH2Cl2 with stirring, stirred for 10 min; water layer sepd., org. layer washed with cold H2O and brine, dried with MgSO4, evapd. in vac., recrystd. from C6H6;
References:
Brown, Herbert C.;Bhat;Somayaji, Vishwanatha [Organometallics,1983,vol. 2,# 10,p. 1311 - 1316]
                        
                        157945-83-0
                        
                        
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                        86595-37-1
                        
                        
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                        917-92-0
                        
                        
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                        $23.00/1g
                        
                    
                        
                        86595-37-1
                        
                        
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                        $45.00/100mg
                        
                    
                        
                        55671-55-1
                        
                        
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                        917-92-0
                        
                        
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                        7732-18-5
                        
                        
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                        $13.50/100ML
                        
                    
                        
                        86595-37-1
                        
                        
                        70 suppliers
                        
                        
                        
                        $45.00/100mg
                        
                    
                        
                        55671-55-1
                        
                        
                        59 suppliers
                        
                        
                        
                        $60.00/10g
                        
                    
                        
                        917-92-0
                        
                        
                        344 suppliers
                        
                        
                        
                        $23.00/1g
                        
                    
                        
                        86595-37-1
                        
                        
                        70 suppliers
                        
                        
                        
                        $45.00/100mg