ChemicalBook CAS DataBase List 3,3-DIMETHYL-1-BUTENYLBORONIC ACID

3,3-DIMETHYL-1-BUTENYLBORONIC ACID synthesis

5synthesis methods

Product Name:3,3-DIMETHYL-1-BUTENYLBORONIC ACID
CAS Number:86595-37-1
Molecular formula:C6H13BO2
Molecular Weight:127.98

Boron, dibromo[(1E)-3,3-dimethyl-1-butenyl][thiobis[methane]]-, (T-4)- (9CI)

72228-60-5
0 suppliers
inquiry

86595-37-1
63 suppliers
$45.00/100mg

Yield:86595-37-1 93%

Reaction Conditions:

with water in diethyl ether;dichloromethane;under N2; to excess of H2O in Et2O added cooled (0 °C) soln. of B complex in CH2Cl2 with stirring, stirred for 10 min; water layer sepd., org. layer washed with cold H2O and brine, dried with MgSO4, evapd. in vac., recrystd. from C6H6;

References:

Brown, Herbert C.;Bhat;Somayaji, Vishwanatha [Organometallics,1983,vol. 2,# 10,p. 1311 - 1316]