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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 3,3-DIMETHYLPIPERIDINE
1193-12-0

3,3-DIMETHYLPIPERIDINE synthesis

6synthesis methods
2,2-Dimethylglutaric acid

681-57-2
179 suppliers
$22.00/1g

3,3-DIMETHYLPIPERIDINE

1193-12-0
63 suppliers
$45.00/50mg

-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: thionyl chloride / 5 h / Heating
2.1: 1,2-dimethoxy-ethane / 15 h / Heating
2.2: 8 h / 200 °C
3.1: 80 percent / LiAlH4 / tetrahydrofuran / 24 h / Heating
4.1: 54 percent / hydrogen / Pd/C / methanol / 20 °C

References:

Berardi, Francesco;Ferorelli, Savina;Colabufo, Nicola Antonio;Leopoldo, Marcello;Perrone, Roberto;Tortorella, Vincenzo [Bioorganic and Medicinal Chemistry,2001,vol. 9,# 5,p. 1325 - 1335]

Piperidine, 3,3-dimethyl-1-(phenylmethyl)-

125943-36-4
1 suppliers
inquiry

3,3-DIMETHYLPIPERIDINE

1193-12-0
63 suppliers
$45.00/50mg

References
2,2 DIMETHYL-4-CYANOBUTYRALDEHYDE

6140-61-0
31 suppliers
inquiry

3,3-DIMETHYLPIPERIDINE

1193-12-0
63 suppliers
$45.00/50mg

References
2,6-Piperidinedione, 3,3-dimethyl-

1194-33-8
7 suppliers
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3,3-DIMETHYLPIPERIDINE

1193-12-0
63 suppliers
$45.00/50mg

References
PENTANEDIOYL DICHLORIDE,2,2-DIMETHYL-

133003-98-2
2 suppliers
inquiry

3,3-DIMETHYLPIPERIDINE

1193-12-0
63 suppliers
$45.00/50mg

References

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