3-(4-chlorophenyl)-3-hydroxypropanoic Acid synthesis
- Product Name:3-(4-chlorophenyl)-3-hydroxypropanoic Acid
- CAS Number:25209-46-5
- Molecular formula:C9H9ClO3
- Molecular Weight:200.62
Yield:25209-46-5 69%
Reaction Conditions:
Stage #1: acetic acidwith n-butyllithium;1,3,3-trimethyl-6-azabicyclo[3.2.1]octane in tetrahydrofuran at -78 - 0;
Stage #2: 4-chlorobenzaldehyde in tetrahydrofuran at 20; for 1 h;
References:
Parra, Margarita;Sotoca, Enrique;Gil, Salvador [European Journal of Organic Chemistry,2003,# 8,p. 1386 - 1388]
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