3,4-Dimethoxymethamphetamine (hydrochloride) synthesis
1synthesis methods
- Product Name:3,4-Dimethoxymethamphetamine (hydrochloride)
- CAS Number:70932-18-2
- Molecular formula:C12H20ClNO2
- Molecular Weight:245.7457
Yield:70932-18-2 58%
Reaction Conditions:
Stage #1: 3,4-dimethoxyphenylacetone;methylamine in methanol at 20; for 0.5 h;
Stage #2: with hydrogenchloride;sodium cyanoborohydride in methanol at 20; pH=4 - 6; for 72 h;Further stages.;
References:
Montgomery;Buon;Eibauer;Guiry;Keenan;McBean [British Journal of Pharmacology,2007,vol. 152,# 7,p. 1121 - 1130]