3,4-dimethylpyridine-2-carboxylic acid synthesis

Yield:1448776-76-8 71%

Reaction Conditions:

with sulfur tetrafluoride;hydrogen fluoride at 85; for 24 h;Autoclave;Inert atmosphere;

References:

Alekseenko, Anatoliy N.;Bugera, Maksym Ya.;Gerus, Igor I.;Kiriakov, Oleksandr;Klipkov, Anton A.;Mykhailiuk, Pavel K.;Pustovit, Yurii;Razhyk, Bohdan;Semenov, Sergey;Starova, Viktoriia S.;Tananaiko, Oksana Yu.;Tarasenko, Karen;Tolmachev, Andrei A.;Trofymchuk, Serhii;Zaporozhets, Olga A. [Journal of Organic Chemistry,2020,vol. 85,# 5,p. 3110 - 3124]